7-Acetoxyheptanal, 7-(2-tetrahydropyranyloxy)heptanal and 8-(2-tetrahydropyranyloxy)octanal were prepared, in good yields, from 7-nitroheptanol and 8-nitrooctanol, via conversion of alcohol, to the corresponding acetate or tetrahydropyranyl derivative, then transformation of the nitro group into aldehyde, by the Nef reaction.
ω-Nitroalcohols as Precursors of Aldehydes ω-Functionalized: A new Synthesis of 7-Acetoxyheptanal 7-(2-Tetrahydropyranyloxy) heptanal and 8-(2-Tetrahydropyranyloxy) octanal.”
BALLINI, Roberto;MARCANTONI, Enrico;PETRINI, Marino
1992-01-01
Abstract
7-Acetoxyheptanal, 7-(2-tetrahydropyranyloxy)heptanal and 8-(2-tetrahydropyranyloxy)octanal were prepared, in good yields, from 7-nitroheptanol and 8-nitrooctanol, via conversion of alcohol, to the corresponding acetate or tetrahydropyranyl derivative, then transformation of the nitro group into aldehyde, by the Nef reaction.File in questo prodotto:
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